Both teams finished the series tied at 1-3 win-loss record behind the undefeated Ponce and will meet on Thursday in Cabo Rojo in a do-or-die contest for the spot in the semifinals.
Sarai Alvarez led Mayaguez Indios with 21 points, followed by Kim Willoughby who contributed 17 points in the victory.
In the other match in Series A, Juncos kept their unbeaten record at 3-0 following a crushing straight-set (25-13, 25-11, 25-7) over the eliminated Carolina (0-4).
Juncos can secure the top spot of the Series with just winning a set against the visiting Caguas that need a 3-0 victory with a difference of more than 15 points to finish in first place.
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